Double kettle automatic reaction calorimeter

CTA-1000D

CTA-1000D double kettle automatic reaction calorimeter is a professional test instrument that simulates the specific process of chemical reaction on a liter scale, measures and controls important process variables. It is an automatic reaction calorimeter under laboratory conditions.

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Product info

CTA-1000D double kettle automatic reaction calorimeter is a professional test instrument that simulates the specific process of chemical reaction on a liter scale, measures and controls important process variables. It is an automatic reaction calorimeter under laboratory conditions.


Product Introduction

CTA-1000D dual -reactor automatic reaction calorimeter can simulate the real situation of batch or semi-batch reactions in factories, and is widely used in reaction process design, process optimization and amplification, process safety assessment, etc. in the fields of fine chemicals, pharmaceuticals, and third-party safety assessment. The instrument is designed mainly for diversified process development and hazard assessment needs. It can adapt to both normal pressure and pressurized reactions, and meet the needs of corrosive material testing. The dual- reactor shares an oil bath and a central controller. The oil circuit realizes rapid switching between the two reactors through valves . There is no need to disassemble the oil circuit to drain the silicone oil in the jacket. The operation is simple and fast, and the instrument is highly integrated.

 

Features

1) It has three calorimetric methods: heat flow, power compensation, and reflow. Users can choose according to their needs

2) Support multiple operation modes such as isothermal, constant temperature, scanning, etc.

3) Optional atmospheric pressure kettle and high pressure kettle or atmospheric pressure kettle and medium pressure kettle

4) The two kettles are fixed by a stand, sharing the oil bath, central control and reflux device, etc., with high integration

5) The double kettles switch the jacket oil circuit through valves, which eliminates the need for disassembly and repeated oil heating, making the operation simple and fast

6) High-power heating and cooling units, fast temperature control response speed, high heat release measurement accuracy

7) It has automatic feeding control for gas, liquid and other materials, and can measure by mass, volume or pressure

8) Accurately measure and obtain process safety related data such as reaction heat flow, reaction enthalpy, conversion rate, sample specific heat capacity, adiabatic temperature rise, and the maximum temperature that the out-of-control system can reach.

9) Chinese software platform, built-in hardware database compatible with more peripherals with different characteristics, flexible programming of experimental processes, real-time monitoring of key data of the reaction process, and online modification of experimental processes and parameters

10) Real-time display of test status such as kettle temperature, jacket temperature, feed mass, stirring speed, pressure, inlet/exhaust speed, pH, inlet and outlet temperatures of the reflux device, etc.

11) Key parameters and status safety thresholds can be set. When the reaction is out of control, "one-click" rapid cooling, abnormal state alarm and automatic shutdown can be performed to effectively ensure safety.

12) Automatically generate and save charts and data, and export experimental analysis reports

 



MODEL

CTA-1000D

Calorimetric method

Heat flow method, power compensation method (optional), reflow method (optional)

temperature control

 

Kettle body temperature range

-25~200

Oil bath temperature range

-45~250

control method

Isothermal, Constant Temperature, Scanning

Temperature resolution

1.0mK

Sample temperature control precision

±0.1K

Silicone oil circulation speed

35L/min~76L/min

Power Control

 

Driver voltage range

0~50VDC

Driver maximum current

3.0A

Heater maximum power

120W

Atmospheric pressure glass reactor (optional)

 

Reactor volume

1000mL, other volumes can be customized

Work Pressure

Atmospheric pressure

Reactor material

Glass

Medium pressure glass reactor (optional)

 

Reactor volume

1000mL, other volumes can be customized

Work Pressure

0.6MPa or 1.2MPa

Reactor body material

Glass

Reactor cover material

316L stainless steel or Hastelloy

High pressure metal reactor (optional)

 

Reactor volume

1000mL, other volumes can be customized

Work Pressure

10MPa

Reactor material

316L stainless steel or Hastelloy

Mixer

 

Maximum speed

2000r/min, 3000r/min optional

Maximum Torque

75N·cm, optional 300N·cm

Stirring paddle type

Anchor or paddle

Material of stirring paddle

PTFE, 316L or Hastelloy

Injection system

 

Injection channel

1 liquid inlet, 1 solid inlet, 1 gas inlet; the inlet can be expanded to 4

Precision balance

Range 3100g, accuracy 0.01g

Injection pump

Medium pressure pump: electromagnetic diaphragm pump, maximum flow rate 2L/h
High pressure pump: precision plunger pump, maximum flow rate 2.4L/h

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